dipyridin-3-yl hexane-1,6-diylbis(MethylcarbaMate)

Base Information

• Chemical Name: dipyridin-3-yl hexane-1,6-diylbis(MethylcarbaMate)
• CAS No.: 95701-58-9
• Molecular Formula: C20H26N4O4
• Molecular Weight: 386.451
• Hs Code.: 2933399090
• Mol file: 95701-58-9.mol

Synonyms:Reaxys ID: 1509149;Distigmine bromide intermediate;dipyridin-3-yl hexane-1,6-diylbis(MethylcarbaMate);Hexamethylenebis[methylcarbamic acid] di-3-pyridyl ester;Carbamic acid, N,N'-1,6-hexanediylbis[N-methyl-, C,C'-di-3-pyridinyl ester

Chemical Property of dipyridin-3-yl hexane-1,6-diylbis(MethylcarbaMate)

Chemical Property:

• Boiling Point: 542.0±50.0 °C(Predicted)
• PKA: 4.29±0.10(Predicted)
• PSA: 84.86000
• Density: 1.186±0.06 g/cm3(Predicted)
• LogP: 3.59840
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Di(pyridin-3-yl)hexane-1,6-diylbis(methylcarbamate) 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dipyridin-3-yl hexane-1,6-diylbis(MethylcarbaMate)

There total 2 articles about dipyridin-3-yl hexane-1,6-diylbis(MethylcarbaMate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-HYDROXYPYRIDINE (109-00-2) + N,N'-dimethyl-N,N'-hexanediyl-bis-carbamoyl chloride (99191-71-6) → Methyl-{6-[methyl-(pyridin-3-yloxycarbonyl)-amino]-hexyl}-carbamic acid pyridin-3-yl ester (95701-58-9)

Guidance literature:

With sodium methylate; In 5,5-dimethyl-1,3-cyclohexadiene; at 80 ℃;

Reference yield:

→ Methyl-{6-[methyl-(pyridin-3-yloxycarbonyl)-amino]-hexyl}-carbamic acid pyridin-3-yl ester (95701-58-9)

Guidance literature:

3-Pyridinol, COCl2, H3C-NH-(CH2)6-NH-CH3;

Reference yield:

methyl bromide (74-83-9) + Methyl-{6-[methyl-(pyridin-3-yloxycarbonyl)-amino]-hexyl}-carbamic acid pyridin-3-yl ester (95701-58-9) → BC 51 (15876-67-2)

Guidance literature:

In acetone; at 0 ℃;

upstream raw materials:

3-HYDROXYPYRIDINE

N,N'-dimethyl-N,N'-hexanediyl-bis-carbamoyl chloride

Downstream raw materials:

BC 51

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