3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester

Base Information

Chemical Name:3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester
CAS No.:211936-61-7
Molecular Formula:C₂₇H₂₃N₃O₄S
Molecular Weight:485.563
Hs Code.:

Synonyms:3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester

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Chemical Property of 3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester

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Technology Process of 3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester

There total 4 articles about 3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 211936-60-6
5-Cyano-6-ethoxycarbonylmethylsulfanyl-4-(1H-indol-3-yl)-2-phenyl-nicotinic acid ethyl ester

: 211936-61-7
3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester

Guidance literature:: With potassium hydroxide; In ethanol; for 5h; Heating;
DOI:10.1080/10426509708043543

Reference yield:

: 94-02-0
ethyl 3-oxo-3-phenylpropionate

: 211936-61-7
3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Et₃N, pyridine / ethanol / 6 h / Heating

2: 85 percent / MeONa / methanol / Heating

3: 80 percent / 10percent KOH / ethanol / 5 h / Heating

With pyridine; potassium hydroxide; sodium methylate; triethylamine; In methanol; ethanol;
DOI:10.1080/10426509708043543

Reference yield:

: 2-cyano-3-(1H-indol-3-yl)prop-2-enethioamide

: 211936-61-7
3-Amino-4-(1H-indol-3-yl)-6-phenyl-thieno[2,3-b]pyridine-2,5-dicarboxylic acid diethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Et₃N, pyridine / ethanol / 6 h / Heating

2: 85 percent / MeONa / methanol / Heating

3: 80 percent / 10percent KOH / ethanol / 5 h / Heating

With pyridine; potassium hydroxide; sodium methylate; triethylamine; In methanol; ethanol;
DOI:10.1080/10426509708043543