ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate

Base Information

Chemical Name:ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate
CAS No.:851579-83-4
Molecular Formula:C₂₈H₄₁N₃O₄
Molecular Weight:483.651
Hs Code.:

Synonyms:ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate

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Chemical Property of ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate

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Technology Process of ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate

There total 1 articles about ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 851579-82-3
[5-([(tert-butoxycarbonyl)amino]methyl)-2-methyl-4-(4-methylphenyl)-6-(2-methylpropyl)pyridin-3-yl]methyl methanesulfonate

: 623-33-6
glycine ethyl ester hydrochloride

: 851579-83-4
ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 60 ℃; for 72h;

Reference yield: 99.0%

: 851579-83-4
ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate

: ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetic acid

Guidance literature:: ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate; With sodium hydroxide; ethanol; water; at 80 ℃; for 15h;

With hydrogenchloride; In water;

Reference yield: 2.4%

: 851579-83-4
ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: tert-butyl {[5-[(2,5-dioxo-1-piperazinyl)methyl]-2-isobutyl-6-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}carbamate

Guidance literature:: N-(Benzyloxycarbonyl)glycine; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 20 ℃; for 0.5h;

ethyl ({[5-{[(tert-butoxycarbonyl)amino]methyl}-6-isobutyl-2-methyl-4-(4-methylphenyl)pyridin-3-yl]methyl}amino)acetate; With pyridine; dmap; In tetrahydrofuran; at 0 ℃; for 3h;

With hydrogen; 5%-palladium/activated carbon; In ethanol; at 20 ℃; for 2h;