C₂₃H₂₆BrClN₆O₄S

Base Information

Chemical Name:C₂₃H₂₆BrClN₆O₄S
CAS No.:1353628-72-4
Molecular Formula:C₂₃H₂₆BrClN₆O₄S
Molecular Weight:597.92
Hs Code.:

C<sub>23</sub>H<sub>26</sub>BrClN<sub>6</sub>O<sub>4</sub>S

Synonyms:C₂₃H₂₆BrClN₆O₄S

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Chemical Property of C₂₃H₂₆BrClN₆O₄S

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Technology Process of C₂₃H₂₆BrClN₆O₄S

There total 9 articles about C₂₃H₂₆BrClN₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1225713-29-0
5-bromo-2-(methylsulfonamido)benzoic acid

: 1353628-70-2
C₁₅H₂₀ClN₅O

: 1353628-72-4
C₂₃H₂₆BrClN₆O₄S

Guidance literature:: 5-bromo-2-(methylsulfonamido)benzoic acid; With HATU; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

C₁₅H₂₀ClN₅O; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 203056-27-3
tert-butyl (2S)-2-{[methoxy(methyl)amino]-carbonyl}piperidine-1-carboxylate

: 1353628-72-4
C₂₃H₂₆BrClN₆O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.42 h / -78 - -20 °C / Inert atmosphere

1.2: 3.08 h / -78 - -45 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: sodium methylate / methanol / 5 h / 78 °C

4.1: trichlorophosphate / 3 h / 100 °C

5.1: sodium carbonate / acetonitrile; water / 0.5 h / 20 °C

6.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C

6.2: 18 h / 20 °C

With sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium carbonate; HATU; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 200184-53-8
(S)-1-tert-butyl 2-methyl piperidine-1,2-dicarboxylate

: 1353628-72-4
C₂₃H₂₆BrClN₆O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

1.2: -78 - -40 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: sodium methylate / methanol / 5 h / 78 °C

4.1: trichlorophosphate / 3 h / 100 °C

5.1: sodium carbonate / acetonitrile; water / 0.5 h / 20 °C

6.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C

6.2: 18 h / 20 °C

With sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium carbonate; HATU; trichlorophosphate; In tetrahydrofuran; methanol; hexanes; ethanol; water; N,N-dimethyl-formamide; acetonitrile;