N-(2-PHENYL-PROPYL)-ACETAMIDE

Base Information

• Chemical Name: N-(2-PHENYL-PROPYL)-ACETAMIDE
• CAS No.: 22596-62-9
• Molecular Formula: C11H15 N O
• Molecular Weight: 177.246
• Hs Code.: 2924299090
• Mol file: 22596-62-9.mol

Synonyms:Acetamide,N-(b-methylphenethyl)- (8CI);N-Acetyl-2-phenylpropylamine; N-Acetyl-b-methylphenethylamine; NSC 272274

Chemical Property of N-(2-PHENYL-PROPYL)-ACETAMIDE

Chemical Property:

• Vapor Pressure: 7.36E-05mmHg at 25°C
• Boiling Point: 342.8°Cat760mmHg
• Flash Point: 203.1°C
• PSA: 29.10000
• Density: 0.993g/cm³
• LogP: 2.31710

Purity/Quality:

95% ^*data from raw suppliers

N-(2-Phenylpropyl)acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(2-PHENYL-PROPYL)-ACETAMIDE

There total 13 articles about N-(2-PHENYL-PROPYL)-ACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2-phenylpropylamine (582-22-9) + acetyl chloride (75-36-5) → N-acetyl-β-methylphenethylamine (22596-62-9)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.666667h;

DOI:10.3390/molecules18021869

Reference yield: 74.0%

N-benzhydryl-2-phenylpropan-1-amine + acetic anhydride (108-24-7) → N-acetyl-β-methylphenethylamine (22596-62-9)

Guidance literature:

With 20% palladium hydroxide-activated charcoal; hydrogen; In dichloromethane; at 40 ℃; under 18751.9 Torr;

DOI:10.1002/adsc.201900372

Reference yield:

2-phenylpropylamine (582-22-9) + acetic anhydride (108-24-7) → N-acetyl-β-methylphenethylamine (22596-62-9)

Guidance literature:

In dichloromethane; at 0 - 20 ℃; for 8.5h;

upstream raw materials:

N-allylacetamide

benzene

2-phenylpropylamine

acetyl chloride

Downstream raw materials:

1,4-dimethyl-3,4-dihydroisoquinoline

2-(2-phenylpropyl)-1H-isoindole-1,3(2H)-dione

N-[2-(4-nitrophenyl)propyl]acetamide

1,4-Dimethyl-isochinolin

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