pimelic acid chloride monobenzyl ester

Base Information

Chemical Name:pimelic acid chloride monobenzyl ester
CAS No.:78582-38-4
Molecular Formula:C₁₄H₁₇ClO₃
Molecular Weight:268.74
Hs Code.:

Synonyms:pimelic acid chloride monobenzyl ester

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Chemical Property of pimelic acid chloride monobenzyl ester

Chemical Property:

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Technology Process of pimelic acid chloride monobenzyl ester

There total 4 articles about pimelic acid chloride monobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15513-04-9
pimelic acid monobenzyl ester

: 78582-38-4
pimelic acid chloride monobenzyl ester

Guidance literature:: With oxalyl dichloride; In dichloromethane; at 25 ℃; for 2h;

Reference yield:

: 142-79-0
pimeloyl chloride

: 100-51-6,185532-71-2
benzyl alcohol

: 78582-38-4
pimelic acid chloride monobenzyl ester

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2005.02.065

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 78582-38-4
pimelic acid chloride monobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 5,5-dimethyl-1,3-cyclohexadiene / 2 h / 140 °C

1.2: 12 h / 60 °C

2.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1.25 h / 0 - 20 °C

With oxalyl dichloride; acetic anhydride; N,N-dimethyl-formamide; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1002/cmdc.201200350