(2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine

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Chemical Name:(2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine
CAS No.:1234804-85-3
Molecular Formula:C₃₁H₃₇NO₄Si
Molecular Weight:515.725
Hs Code.:

Synonyms:(2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine

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Chemical Property of (2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine

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Technology Process of (2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine

There total 6 articles about (2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1234804-84-2
(2R,5S)-1-benzyloxycarbonyl-5-(2-(tert-butyldiphenylsilyloxy)ethyl)-2-(methoxycarbonyl)pyrrolidine

: 1234804-85-3
(2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.3998/ark.5550190.0011.402

Reference yield:

: C₁₅H₁₉NO₅

: 1234804-85-3
(2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 0.5 h / 0 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / 0 °C / Inert atmosphere

3: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere

With 1H-imidazole; diisobutylaluminium hydride; In ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.3998/ark.5550190.0011.402

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1234804-85-3
(2S,5R)-benzyloxycarbonyl-2-(2-(tert-butyldiphenylsilyloxy)ethyl)-5-formylpyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 0 °C / Inert atmosphere

2: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere

With 1H-imidazole; diisobutylaluminium hydride; In N,N-dimethyl-formamide; toluene;
DOI:10.3998/ark.5550190.0011.402