Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester

Base Information

• Chemical Name: Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester
• CAS No.: 201055-38-1
• Molecular Formula: C₂₂H₃₃NO₅
• Molecular Weight: 391.508

Synonyms:Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester

Chemical Property of Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester

There total 5 articles about Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,3S)-3-propyl-2-oxiranemethanol (89321-71-1) → Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester (201055-38-1)

Guidance literature:

Multi-step reaction with 3 steps

1: Ti(O-i-Pr)4 / tetrahydrofuran

2: NaHCO₃

With titanium(IV) isopropylate; sodium hydrogencarbonate; In tetrahydrofuran;

DOI:10.1016/S0040-4039(97)10367-7

Reference yield:

benzylamine (100-46-9) → Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester (201055-38-1)

Guidance literature:

Multi-step reaction with 3 steps

1: Ti(O-i-Pr)4 / tetrahydrofuran

2: NaHCO₃

With titanium(IV) isopropylate; sodium hydrogencarbonate; In tetrahydrofuran;

DOI:10.1016/S0040-4039(97)10367-7

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → Carbonic acid (R)-2-(benzyl-tert-butoxycarbonyl-amino)-1-vinyl-pentyl ester ethyl ester (201055-38-1)

Guidance literature:

Multi-step reaction with 2 steps

1: NaHCO₃

With sodium hydrogencarbonate;

DOI:10.1016/S0040-4039(97)10367-7

upstream raw materials:

vinyl magnesium bromide

chloroformic acid ethyl ester

di-tert-butyl dicarbonate

(2S,3S)-3-propyl-2-oxiranemethanol

Downstream raw materials:

Benzyl-((1R,2R,3R)-3-hydroxy-1-propyl-2-vinyl-pentyl)-carbamic acid tert-butyl ester

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