C₇₆H₁₃₀O₁₃Si₃

Base Information

Chemical Name:C₇₆H₁₃₀O₁₃Si₃
CAS No.:880876-74-4
Molecular Formula:C₇₆H₁₃₀O₁₃Si₃
Molecular Weight:1336.12
Hs Code.:

C<sub>76</sub>H<sub>130</sub>O<sub>13</sub>Si<sub>3</sub>

Synonyms:C₇₆H₁₃₀O₁₃Si₃

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Chemical Property of C₇₆H₁₃₀O₁₃Si₃

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Technology Process of C₇₆H₁₃₀O₁₃Si₃

There total 25 articles about C₇₆H₁₃₀O₁₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 862465-79-0
C₇₆H₁₂₈O₁₃Si₃

: 880876-74-4
C₇₆H₁₃₀O₁₃Si₃

Guidance literature:: With zinc(II) tetrahydroborate; In diethyl ether; dichloromethane; at 0 ℃; for 4h;
DOI:10.1021/ol051225n

Reference yield:

: 862465-63-2
tert-butyl 2-{(6S,4R)-2-(4-methoxyphenyl)-6-[(phenylmethoxy)methyl]-1,3-dioxan-4-yl}acetate

: 880876-74-4
C₇₆H₁₃₀O₁₃Si₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: 89 percent / Raney Nickel; H₂ / ethanol / 3 h / 20 °C / 760 Torr

2.1: 90 percent / imidazole / CH₂Cl₂ / 16 h / 20 °C

3.1: 87 percent / isopropylmagnesium chloride / tetrahydrofuran / -30 - 0 °C

4.1: 93 percent / MgBr₂*Et₂O; n-tributyltin chloride / CH₂Cl₂ / 5 h / 20 °C

5.1: 89 percent / tetrahydrofuran / 2 h / 0 °C

6.1: EtBOMe; NaBH₄ / tetrahydrofuran; methanol / 9 h / -78 °C

6.2: H₂O₂ / methanol; tetrahydrofuran; H₂O / -78 - 20 °C

7.1: 3.80 g / PPTs / CH₂Cl₂ / 1 h / 20 °C

8.1: 86 percent / pyridine; O₃; Sudan III / Ph₃P / CH₂Cl₂; methanol / -78 - 20 °C

9.1: n-Bu₂BOTf; Et₃N / CH₂Cl₂ / 1.5 h / -78 - 0 °C

9.2: 93 percent / CH₂Cl₂ / 2 h / -78 - 0 °C

10.1: 73 percent / AlMe₃ / tetrahydrofuran / 10 h / -10 - 0 °C

11.1: 82 percent / 2,6-lutidine / CH₂Cl₂ / 3 h / -78 °C

12.1: 88 percent / DIBAL-H / CH₂Cl₂; toluene / 3 h / -78 °C

13.1: chlorodicycloheylborane; Et₃N / diethyl ether / 1.67 h / -78 - 0 °C

13.2: diethyl ether / 21 h / -78 - -20 °C

13.3: 40 percent / H₂O₂ / diethyl ether; methanol; H₂O / 1 h / 0 °C / pH 7

14.1: 70 percent / Zn(BH₄)2 / CH₂Cl₂; diethyl ether / 4 h / 0 °C

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; sodium tetrahydroborate; zinc(II) tetrahydroborate; oil scarlet; di-n-butylboryl trifluoromethanesulfonate; dicyclohexylboron chloride; tributyltin chloride; hydrogen; trimethylaluminum; isopropylmagnesium chloride; pyridinium p-toluenesulfonate; nickel; diisobutylaluminium hydride; ozone; triethylamine; magnesium bromide; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene;
DOI:10.1021/ol051225n

Reference yield:

: 862465-64-3
2-((6S,4R)-6-{[1,1-bis(1-methylethyl)-2-methyl-1-silapropoxy]methyl}-2-(4-methoxyphenyl)(1,3-dioxan-4-yl))-N-methoxy-N-methylacetamide

: 880876-74-4
C₇₆H₁₃₀O₁₃Si₃

Guidance literature:: Multi-step reaction with 11 steps

1.1: 93 percent / MgBr₂*Et₂O; n-tributyltin chloride / CH₂Cl₂ / 5 h / 20 °C

2.1: 89 percent / tetrahydrofuran / 2 h / 0 °C

3.1: EtBOMe; NaBH₄ / tetrahydrofuran; methanol / 9 h / -78 °C

3.2: H₂O₂ / methanol; tetrahydrofuran; H₂O / -78 - 20 °C

4.1: 3.80 g / PPTs / CH₂Cl₂ / 1 h / 20 °C

5.1: 86 percent / pyridine; O₃; Sudan III / Ph₃P / CH₂Cl₂; methanol / -78 - 20 °C

6.1: n-Bu₂BOTf; Et₃N / CH₂Cl₂ / 1.5 h / -78 - 0 °C

6.2: 93 percent / CH₂Cl₂ / 2 h / -78 - 0 °C

7.1: 73 percent / AlMe₃ / tetrahydrofuran / 10 h / -10 - 0 °C

8.1: 82 percent / 2,6-lutidine / CH₂Cl₂ / 3 h / -78 °C

9.1: 88 percent / DIBAL-H / CH₂Cl₂; toluene / 3 h / -78 °C

10.1: chlorodicycloheylborane; Et₃N / diethyl ether / 1.67 h / -78 - 0 °C

10.2: diethyl ether / 21 h / -78 - -20 °C

10.3: 40 percent / H₂O₂ / diethyl ether; methanol; H₂O / 1 h / 0 °C / pH 7

11.1: 70 percent / Zn(BH₄)2 / CH₂Cl₂; diethyl ether / 4 h / 0 °C

With pyridine; 2,6-dimethylpyridine; sodium tetrahydroborate; zinc(II) tetrahydroborate; oil scarlet; di-n-butylboryl trifluoromethanesulfonate; dicyclohexylboron chloride; tributyltin chloride; trimethylaluminum; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; ozone; triethylamine; magnesium bromide; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene;
DOI:10.1021/ol051225n