C₁₅H₃₁NO₃S₂

Base Information

• Chemical Name: C₁₅H₃₁NO₃S₂
• CAS No.: 1263416-47-2
• Molecular Formula: C₁₅H₃₁NO₃S₂
• Molecular Weight: 337.548
• Mol file: 1263416-47-2.mol

Synonyms:C₁₅H₃₁NO₃S₂

Chemical Property of C₁₅H₃₁NO₃S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₃₁NO₃S₂

There total 3 articles about C₁₅H₃₁NO₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl methyl sulfone (14094-12-3) + N-cyclohexylidene-2-methylpropane-2-sulfinamide (729559-16-4) → C15H31NO3S2 (1263416-47-2)

Guidance literature:

tert-butyl methyl sulfone; With n-butyllithium; In hexane; tert-butyl methyl ether; at 0 - 3 ℃; for 3.5h; Industry scale;

N-cyclohexylidene-2-methylpropane-2-sulfinamide; In hexane; tert-butyl methyl ether; at 2 ℃; for 1.5h; Industry scale;

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → C15H31NO3S2 (1263416-47-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 4 h / 60 °C / Industry scale

2.1: n-butyllithium / hexane; tert-butyl methyl ether / 3.5 h / 0 - 3 °C / Industry scale

2.2: 1.5 h / 2 °C / Industry scale

With titanium(IV) tetraethanolate; n-butyllithium; In tetrahydrofuran; hexane; tert-butyl methyl ether;

Reference yield:

tert-butyl methyl sulphide (6163-64-0) → C15H31NO3S2 (1263416-47-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium tungstate; dihydrogen peroxide / water / 0.25 h / 22 - 30 °C / Inert atmosphere; Industry scale

2.1: n-butyllithium / hexane; tert-butyl methyl ether / 3.5 h / 0 - 3 °C / Industry scale

2.2: 1.5 h / 2 °C / Industry scale

With sodium tungstate; n-butyllithium; dihydrogen peroxide; In hexane; tert-butyl methyl ether; water;

upstream raw materials:

cyclohexanone

tert-butyl methyl sulphide

tert-butyl methyl sulfone

N-cyclohexylidene-2-methylpropane-2-sulfinamide

Downstream raw materials:

C₁₈H₂₇NO₄S

C₁₁H₂₃NO₂S

C₃₆H₆₃N₅O₇S

C₂₆H₄₅N₃O₆S