methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate

Base Information

Chemical Name:methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate
CAS No.:1200398-08-8
Molecular Formula:C₁₂H₁₀Cl₂N₂O₂S₂
Molecular Weight:349.262
Hs Code.:

Synonyms:methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate

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Technology Process of methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate

There total 4 articles about methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1190213-40-1
C₁₃H₁₅Cl₂N₃O₃S

: 1200398-08-8
methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate

Guidance literature:: With thionyl chloride; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1002/cbdv.200900197

Reference yield:

: 2632-10-2
2-bromo-1-(3,4-dichlorophenyl)ethanone

: 1200398-08-8
methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / ethanol / 12 h / 20 °C

2.1: sodium acetate / ethanol / 1 h / Reflux

2.2: Reflux

3.1: thionyl chloride / dichloromethane / 20 °C / Cooling with ice

With thionyl chloride; sodium acetate; sodium carbonate; In ethanol; dichloromethane;
DOI:10.1002/cbdv.200900197

Reference yield:

: 1152629-53-2
methyl 3-{[2-(3,4-dichlorophenyl)-2-oxoethyl]sulfanyl}propanoate

: 1200398-08-8
methyl 3-{[4-(3,4-dichlorophenyl)-1,2,3-thiadiazol-5-yl]sulfanyl}propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / ethanol / 1 h / Reflux

1.2: Reflux

2.1: thionyl chloride / dichloromethane / 20 °C / Cooling with ice

With thionyl chloride; sodium acetate; In ethanol; dichloromethane;
DOI:10.1002/cbdv.200900197