Technology Process of C35H32O7
There total 5 articles about C35H32O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
at 20 ℃;
for 72h;
Inert atmosphere;
DOI:10.1039/c0cc04979d
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; sodium nitrite / water / 2 h / 0 °C / Inert atmosphere
1.2: 12 h / 0 - 20 °C / Inert atmosphere
2.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / 12 h / 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere
3.2: Cooling with ice; Inert atmosphere
4.1: pyridine / 12 h / 20 °C / Inert atmosphere
5.1: pyridine; dmap / 72 h / 20 °C / Inert atmosphere
With
piperidine; pyridine; hydrogenchloride; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium aluminium tetrahydride; triphenylphosphine; sodium nitrite;
In
tetrahydrofuran; water;
2.1: Sonogashira coupling;
DOI:10.1039/c0cc04979d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 60 °C / Inert atmosphere
1.2: Cooling with ice; Inert atmosphere
2.1: pyridine / 12 h / 20 °C / Inert atmosphere
3.1: pyridine; dmap / 72 h / 20 °C / Inert atmosphere
With
pyridine; dmap; lithium aluminium tetrahydride;
In
tetrahydrofuran;
DOI:10.1039/c0cc04979d
