2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane

Base Information

Chemical Name:2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane
CAS No.:900146-76-1
Molecular Formula:C₁₇H₂₂ClNO₃
Molecular Weight:323.82
Hs Code.:

Synonyms:2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane

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Chemical Property of 2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane

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Technology Process of 2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane

There total 5 articles about 2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 146725-33-9
O 374

: 540-51-2
2-bromoethanol

: 900146-76-1
2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane

Guidance literature:: With triethylamine; In acetonitrile; at 80 ℃; for 5h; Inert atmosphere;
DOI:10.1002/jlcr.3181

Reference yield:

: 130342-80-2
2β-carbomethoxy-3β-(4-chlorophenyl)tropane

: 900146-76-1
2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane

Guidance literature:: Multi-step reaction with 3 steps

1: 2 h / 120 °C

2: acetic acid; zinc / 16 h / 20 °C

3: triethylamine / acetonitrile / 5 h / 80 °C / Inert atmosphere

With acetic acid; triethylamine; zinc; In acetonitrile;
DOI:10.1002/jlcr.3181

Reference yield:

: 481-37-8
ecgonine

: 900146-76-1
2β-carbomethoxy-3β-(4-chlorophenyl)-8-(2-hydroxyethyl)nortropane

Guidance literature:: Multi-step reaction with 6 steps

1.1: trichlorophosphate

2.1: hydrogenchloride

3.1: diethyl ether / -45 °C

3.2: -78 °C

4.1: 2 h / 120 °C

5.1: acetic acid; zinc / 16 h / 20 °C

6.1: triethylamine / acetonitrile / 5 h / 80 °C / Inert atmosphere

With hydrogenchloride; acetic acid; triethylamine; zinc; trichlorophosphate; In diethyl ether; acetonitrile; 2.1: |Fischer-Speier Esterification;
DOI:10.1002/jlcr.3181