Technology Process of C31H40FN5O8
There total 10 articles about C31H40FN5O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C33H44FN5O8;
With
water; sodium hydroxide;
In
methanol;
at 30 ℃;
for 0.5h;
With
hydrogenchloride;
In
water;
pH=2 - 3;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / -20 - 20 °C / Inert atmosphere
2.1: water; lithium hydroxide monohydrate / methanol / 16 h / 20 °C
2.2: pH 4 - 5 / Acidic aqueous solution
3.1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / 0 - 20 °C
3.2: 0 °C
4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / -5 - 10 °C
5.1: sodium hydroxide; water / methanol / 0.5 h / 30 °C
5.2: pH 2 - 3
With
lithium hydroxide monohydrate; di-isopropyl azodicarboxylate; dimethylsulfide borane complex; water; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; methanol;
1.1: Mitsunobu reaction / 4.1: Mitsunobu reaction;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 - -65 °C / Molecular sieve
1.2: 3 h / -65 °C
2.1: hydrazine / tetrahydrofuran; methanol / 2 h / 10 - 20 °C
3.1: N-Bromosuccinimide / 20 - 30 °C
4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / -5 - 10 °C
5.1: sodium hydroxide; water / methanol / 0.5 h / 30 °C
5.2: pH 2 - 3
With
N-Bromosuccinimide; n-butyllithium; di-isopropyl azodicarboxylate; water; triphenylphosphine; sodium hydroxide; hydrazine;
In
tetrahydrofuran; methanol;
4.1: Mitsunobu reaction;
