1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide

Base Information

• Chemical Name: 1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide
• CAS No.: 675609-94-6
• Molecular Formula: C₇₂H₅₄I₄N₂O₈
• Molecular Weight: 1582.85
• Mol file: 675609-94-6.mol

Synonyms:1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide

Chemical Property of 1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide

There total 2 articles about 1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

p-Iodophenol (540-38-5) + N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid diimide (112078-00-9) → 1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide (675609-94-6)

Guidance literature:

With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 15h;

DOI:10.1002/chem.200304994

Reference yield: 80.0%

p-Iodophenol (540-38-5) + N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide (861853-38-5) → 1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide (675609-94-6)

Guidance literature:

With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 15h; Inert atmosphere;

DOI:10.1080/00397910903013754

Reference yield: 91.0%

trimethylsilylacetylene (1066-54-2) + 1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide (675609-94-6) → 1,6,7,12-tetrakis[4-(trimethylsilylethynyl)phenoxy]-N,N'-(2,6-diisopropylphenyl)perylene-3,4,9,10-tetracarboxdiimide

Guidance literature:

With copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; at 20 ℃; for 15h;

DOI:10.1002/chem.200304994

upstream raw materials:

p-Iodophenol

N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrachloroperylene-3,4:9,10-tetracarboxylic acid diimide

N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide