N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide

Base Information

Chemical Name:N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide
CAS No.:861853-38-5
Molecular Formula:C₄₈H₃₈Br₄N₂O₄
Molecular Weight:1026.46
Hs Code.:

Synonyms:N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide

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Chemical Property of N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide

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Technology Process of N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide

There total 1 articles about N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 861853-38-5
N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 12 h / 20 °C

1.2: 85 - 110 °C

2.1: propionic acid / 10 h / 140 °C / Inert atmosphere

With sulfuric acid; In propionic acid;
DOI:10.1080/00397910903013754

Reference yield: 80.0%

: 540-38-5
p-Iodophenol

: 861853-38-5
N,N'-bis(2,6-diisopropylphenyl)-1,6,7,12-tetrabromoperylene-3,4:9,10-tetracarboxylic acid bisimide

: 675609-94-6
1,6,7,12-tetrakis(4-iodophenoxy)-N,N'-(2,6-diisopropylphenyl)perylenetetracarboxy-3,4:9,10-diimide

Guidance literature:: With potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 80 ℃; for 15h; Inert atmosphere;
DOI:10.1080/00397910903013754