resorthiomycin dimethyl ether

Base Information

Chemical Name:resorthiomycin dimethyl ether
CAS No.:245368-65-4
Molecular Formula:C₁₆H₂₄O₄S
Molecular Weight:312.43
Hs Code.:

Synonyms:resorthiomycin dimethyl ether

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Chemical Property of resorthiomycin dimethyl ether

Chemical Property:

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Technology Process of resorthiomycin dimethyl ether

There total 9 articles about resorthiomycin dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 245368-64-3
2,4-dimethoxy-3,6-dimethyl-5-(3-oxo-butyl)-thiobenzoic acid S-methyl ester

: 245368-65-4
resorthiomycin dimethyl ether

Guidance literature:: With sodium tetrahydroborate; In methanol;
DOI:10.1016/S0040-4039(99)01015-1

Reference yield:

: 4707-47-5
2,4-dihydroxy-3,6-dimethyl-benzoic acid methyl ester

: 245368-65-4
resorthiomycin dimethyl ether

Guidance literature:: Multi-step reaction with 9 steps

1: 90 percent / CF₃COOH

2: 89 percent / K₂CO₃ / acetone

3: 71 percent / NaOH

4: 88 percent / Mg / methanol

5: 79 percent / KOH / methanol; H₂O

6: SOCl₂ / benzene

7: KSH; H⁽¹⁺⁾ / benzene

8: K₂CO₃ / acetone

9: 90 percent / NaBH₄ / methanol

With potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; hydrogen cation; potassium carbonate; potassium hydrosulfide; magnesium; trifluoroacetic acid; In methanol; water; acetone; benzene; 1: Formylation / 2: Methylation / 3: Condensation / 4: Reduction / 5: Hydrolysis / 6: Substitution / 7: Substitution / 8: Methylation / 9: Reduction;
DOI:10.1016/S0040-4039(99)01015-1

Reference yield:

: 3187-58-4
methyl orsellinate

: 245368-65-4
resorthiomycin dimethyl ether

Guidance literature:: Multi-step reaction with 11 steps

1: 80 percent / AlCl₃ / diethyl ether

2: 78 percent / Zn(Hg); HCl / methanol

3: 90 percent / CF₃COOH

4: 89 percent / K₂CO₃ / acetone

5: 71 percent / NaOH

6: 88 percent / Mg / methanol

7: 79 percent / KOH / methanol; H₂O

8: SOCl₂ / benzene

9: KSH; H⁽¹⁺⁾ / benzene

10: K₂CO₃ / acetone

11: 90 percent / NaBH₄ / methanol

With hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; thionyl chloride; hydrogen cation; potassium carbonate; potassium hydrosulfide; magnesium; mercury; trifluoroacetic acid; zinc; In methanol; diethyl ether; water; acetone; benzene; 1: Formylation / 2: Reduction / 3: Formylation / 4: Methylation / 5: Condensation / 6: Reduction / 7: Hydrolysis / 8: Substitution / 9: Substitution / 10: Methylation / 11: Reduction;
DOI:10.1016/S0040-4039(99)01015-1