2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene

Base Information

Chemical Name:2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene
CAS No.:893408-44-1
Molecular Formula:C₁₉H₂₃BrO
Molecular Weight:347.295
Hs Code.:

Synonyms:2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene

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Chemical Property of 2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene

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Technology Process of 2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene

There total 2 articles about 2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2432-03-3
4-bromopropofol

: 100-39-0
benzyl bromide

: 893408-44-1
2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 40 ℃; for 12h;
DOI:10.1016/j.tet.2006.01.090

Reference yield:

: 2078-54-8
2,6-diisopropylphenol

: 893408-44-1
2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂; AcOH / 6 h / 20 °C

2: 86 percent / NaH / tetrahydrofuran / 12 h / 40 °C

With bromine; sodium hydride; acetic acid; In tetrahydrofuran;
DOI:10.1016/j.tet.2006.01.090

Reference yield: 73.0%

: 893408-44-1
2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene

: 1360626-50-1
2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylbenzaldehyde

: (4-(benzyloxy)-3,5-diisopropylphenyl)(2-(tert-butyldimethylsilyloxy)-4-methylphenyl)methanol

Guidance literature:: 2-(benzyloxy)-5-bromo-1,3-diisopropylbenzene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

2-{[tert-butyl(dimethyl)silyl]oxy}-4-methylbenzaldehyde; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1002/anie.201606947