7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

Base Information

Chemical Name:7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane
CAS No.:160358-53-2
Molecular Formula:C₅₄H₆₂N₂O₈
Molecular Weight:867.095
Hs Code.:

Synonyms:7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

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Chemical Property of 7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

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Technology Process of 7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

There total 5 articles about 7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 81464-85-9
2,3-Bis(benzyloxy)benzyl bromide

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 160358-53-2
7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

Guidance literature:: With triethylamine; In toluene; for 16.5h; Ambient temperature;
DOI:10.1016/0040-4039(94)80116-9

Reference yield:

: 5779-91-9
2,3-bis(benzyloxy)benzaldehyde

: 160358-53-2
7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / LiAlH₄ / tetrahydrofuran

2: 98 percent / PBr₃ / tetrahydrofuran

3: 78 percent / Et₃N / toluene / 16.5 h / Ambient temperature

With lithium aluminium tetrahydride; phosphorus tribromide; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1016/0040-4039(94)80116-9

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 160358-53-2
7,16-Bis-(2,3-bis-benzyloxy-benzyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadecane

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / ethanol

2: 80 percent / LiAlH₄ / tetrahydrofuran

3: 98 percent / PBr₃ / tetrahydrofuran

4: 78 percent / Et₃N / toluene / 16.5 h / Ambient temperature

With lithium aluminium tetrahydride; phosphorus tribromide; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; toluene;
DOI:10.1016/0040-4039(94)80116-9