3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

Base Information

Chemical Name:3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide
CAS No.:1416973-57-3
Molecular Formula:C₃₇H₅₃ClN₈O₇
Molecular Weight:757.33
Hs Code.:

3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

Synonyms:3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

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Chemical Property of 3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

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Technology Process of 3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

There total 5 articles about 3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76942-92-2
methyl 3,5-diamino-6-chloropyrazine-2-carbonylcarbamimidothioate hydroiodic acid salt

: (1R,2S)-3((2-(4-(4-aminobutyl)phenoxy)ethyl)(hexyl)amino)-1-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propane-1,2-diol acetic acid

: 1416973-57-3
3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; at 20 - 70 ℃; for 2h; Sealed tube;

Reference yield:

: 587880-55-5
{4-[4-(2-tert-Butoxycarbonylaminoethoxy)phenyl]butyl}carbamic acid benzyl ester

: 1416973-57-3
3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

2.1: acetic acid / methanol / 2 h / 20 °C

2.2: 20 °C

2.3: 20 °C

3.1: acetic acid; palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / 760.05 Torr

4.1: N-ethyl-N,N-diisopropylamine / ethanol / 2 h / 20 - 70 °C / Sealed tube

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; ethanol;

Reference yield:

: 587880-59-9
{4-[4-(2-Aminoethoxy)phenyl]butyl}carbamic acid benzyl ester hydrochloride

: 1416973-57-3
3,5-diamino-6-chloro-N-(N-(4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)propyl)(hexyl)amino)ethoxy)phenyl)butyl)carbanmdoyl)pyrazine-2-carboxarnide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / methanol / 2 h / 20 °C

1.2: 20 °C

1.3: 20 °C

2.1: acetic acid; palladium 10% on activated carbon; hydrogen / ethanol / 20 °C / 760.05 Torr

3.1: N-ethyl-N,N-diisopropylamine / ethanol / 2 h / 20 - 70 °C / Sealed tube

With palladium 10% on activated carbon; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; In methanol; ethanol;