2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate

Base Information

• Chemical Name: 2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate
• CAS No.: 1147090-63-8
• Molecular Formula: C₂₆H₃₈N₂O₄
• Molecular Weight: 442.599

Synonyms:2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate

Chemical Property of 2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate

There total 1 articles about 2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

N-methylhomoveratrylamine (3490-06-0) + 1-phenylvinyl N',N'-diisopropylcarbamate (359868-65-8) → 2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate (1147090-63-8)

Guidance literature:

N-methylhomoveratrylamine; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.25h; Inert atmosphere;

1-phenylvinyl N',N'-diisopropylcarbamate; In tetrahydrofuran; hexane; at 0 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2009.01.098

Reference yield: 90.0%

2-(N-3,4-dimethoxyphenethyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate (1147090-63-8) → 1-phenyl-N-methyl-7,8-dimethoxy-1,2,4,5-tetrahydro-3H-benzazepine (20012-08-2)

Guidance literature:

With methanesulfonic acid; trifluoroacetic acid; for 24h; Reflux;

DOI:10.1016/j.tet.2009.01.098

upstream raw materials:

N-methylhomoveratrylamine

1-phenylvinyl N',N'-diisopropylcarbamate

Downstream raw materials:

1-phenyl-N-methyl-7,8-dimethoxy-1,2,4,5-tetrahydro-3H-benzazepine

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