1-Phenylethenyl N,N-bis(1-methylethyl)carbamate

Base Information

Chemical Name:1-Phenylethenyl N,N-bis(1-methylethyl)carbamate
CAS No.:359868-65-8
Molecular Formula:C₁₅H₂₁NO₂
Molecular Weight:247.337
Hs Code.:
DSSTox Substance ID:DTXSID901243117
Nikkaji Number:J1.729.785F

Synonyms:DTXSID901243117;359868-65-8;1-Phenylethenyl N,N-bis(1-methylethyl)carbamate

Suppliers and Price of 1-Phenylethenyl N,N-bis(1-methylethyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenylethenyl N,N-bis(1-methylethyl)carbamate

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:247.157228913
Heavy Atom Count:18
Complexity:283

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)N(C(C)C)C(=O)OC(=C)C1=CC=CC=C1

Technology Process of 1-Phenylethenyl N,N-bis(1-methylethyl)carbamate

There total 2 articles about 1-Phenylethenyl N,N-bis(1-methylethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 19009-39-3
N,N-diisopropylcarbamoyl chloride

: 98-86-2
acetophenone

: 359868-65-8
1-phenylvinyl N',N'-diisopropylcarbamate

Guidance literature:: With pyridine; at 95 ℃; for 144h;
DOI:10.1055/s-2002-20040

Reference yield:

: 145167-88-0
N,N-diisopropyl carbamic acid (1-phenylethyl) ester

: 359868-65-8
1-phenylvinyl N',N'-diisopropylcarbamate

Guidance literature:: With Ph(COD)2BF₄; hydrogen; triphenylphosphine; In dichloromethane;
DOI:10.1021/ol051559c

Reference yield: 91.0%

: 103-67-3
benzyl-methyl-amine

: 359868-65-8
1-phenylvinyl N',N'-diisopropylcarbamate

: 1147090-56-9
2-(N-benzyl-N-methylamino)-1-phenylethyl N',N'-diisopropylcarbamate

Guidance literature:: benzyl-methyl-amine; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.25h; Inert atmosphere;

1-phenylvinyl N',N'-diisopropylcarbamate; In tetrahydrofuran; hexane; at -40 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tet.2009.01.098