trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

Base Information

Chemical Name:trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol
CAS No.:88627-60-5
Molecular Formula:C₂H₂O₄*C₂₆H₂₉NO₃
Molecular Weight:493.557
Hs Code.:

Synonyms:trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

Suppliers and Price of trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

There total 2 articles about trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 621-87-4
3-phenoxy-2-propanone

: 144-62-7,97993-78-7
oxalic acid

: 66361-29-3,116885-88-2
trans-2-amino-6-benzyloxy-1,2,3,4-tetrahydronaphthalen-1-ol

: 88627-60-5
trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

Guidance literature:: With sodium cyanoborohydride; In methanol; ethanol; at 5 ℃;
DOI:10.1248/cpb.31.2329

Reference yield:

: 66361-76-0
2-Amino-6-benzyloxy-3,4-dihydro-2H-naphthalen-1-one; hydrochloride

: 88627-60-5
trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 1.) NaBH₄; 2.) 20percent HCl/EtOH / methanol / 0.5 h / Ambient temperature

2: 70 percent / 1.) NaBH₃CN / methanol; ethanol / 5 °C

With hydrogenchloride; sodium tetrahydroborate; ethanol; sodium cyanoborohydride; In methanol; ethanol;
DOI:10.1248/cpb.31.2329

Reference yield: 86.0%

: 88627-60-5
trans-6-benzyloxy-2-(1-methyl-2-phenoxyethyl)-amino-1,2,3,4-tetrahydronaphthalen-1-ol

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 88627-55-8
trans-5-hydroxy-2-(1-methyl-2-phenoxyethyl)amino-1,2,3,4-tetrahydronaphthalen-1-ol

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; diethyl ether; Ambient temperature;
DOI:10.1248/cpb.31.2329