(S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

Base Information

Chemical Name:(S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate
CAS No.:1449004-76-5
Molecular Formula:C₂₇H₂₉N₃O₇S
Molecular Weight:539.609
Hs Code.:

Synonyms:(S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

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Chemical Property of (S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

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Technology Process of (S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

There total 1 articles about (S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 55871-46-0
benzyl 4-sulfamoylphenylcarbamate

: 2900-27-8
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid

: 1449004-76-5
(S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c3ob40236c

Reference yield: 61.0%

: 1449004-76-5
(S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

: 1449004-13-0
(S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 2h;
DOI:10.1039/c3ob40236c

Reference yield:

: 1449004-76-5
(S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

: 1449004-35-6
2-(4-bromo-2-chlorophenoxy)-N-(4-(N-(N-tert-butoxycarbonyl-L-(2-phenyl)glycyl)sulfamoyl)phenylcarbamothioyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

2: acetone / 20 °C

With palladium 10% on activated carbon; hydrogen; In methanol; acetone;
DOI:10.1039/c3ob40236c