(S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate
CAS No.:1449004-13-0
Molecular Formula:C₁₉H₂₃N₃O₅S
Molecular Weight:405.475
Hs Code.:

Synonyms:(S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

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Chemical Property of (S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

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Technology Process of (S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

There total 3 articles about (S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1449004-76-5
(S)-benzyl-4-(N-(2-(tert-butoxycarbonylamino)-2-phenylacetyl)-sulfamoyl)phenylcarbamate

: 1449004-13-0
(S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 2h;
DOI:10.1039/c3ob40236c

Reference yield:

: 2900-27-8
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid

: 1449004-13-0
(S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1039/c3ob40236c

Reference yield:

: 55871-46-0
benzyl 4-sulfamoylphenylcarbamate

: 1449004-13-0
(S)-tert-butyl 2-(4-aminophenylsulfonamido)-2-oxo-1-phenylethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1039/c3ob40236c