[(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine^(1-))]ClO₄*MeOH

Base Information

• Chemical Name: [(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine^(1-))]ClO₄*MeOH
• CAS No.: 922498-85-9
• Molecular Formula: CH₄O*C₃₅H₃₄N₅NiO*ClO₄
• Molecular Weight: 730.871

Synonyms:[(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine^(1-))]ClO₄*MeOH

Chemical Property of [(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine^(1-))]ClO₄*MeOH

Chemical Property:

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Technology Process of [(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine^(1-))]ClO₄*MeOH

There total 1 articles about [(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine^(1-))]ClO₄*MeOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

methanol (67-56-1) + [(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine)](ClO4)2 → [(N,N-bis-[(6-phenyl-2-pyridyl)methyl]-N-[(6-pivaloylamido-2-pyridyl)methyl]amine(1-))]ClO4*MeOH (922498-85-9)

Guidance literature:

With Me₄NOH*5H₂O; In acetonitrile; under N2 atm. soln. Ni complex in MeCN was added to suspn. Me4NOH*5H2O in MeCN and stirred for 4 h; solvent was removed in vacuo, residue was dissolved in CH2Cl2, filtered through Celite, solvent was removed in vacuo, residue was recrystd. by Et2O diffusion into MeCN-MeOH (2:1); elem. anal.;

DOI:10.1021/ja0601336

upstream raw materials:

methanol

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