Diazoacetylglycine hydrazide

Base Information

• Chemical Name: Diazoacetylglycine hydrazide
• CAS No.: 820-75-7
• Molecular Formula: C4H7 N5 O2
• Molecular Weight: 157.132
• NSC Number: 58404
• UNII: QZ889UKY6W
• DSSTox Substance ID: DTXSID301002371
• Nikkaji Number: J35.142C
• Mol file: 820-75-7.mol

Synonyms:N-diazoacetylglycine hydrazide

Chemical Property of Diazoacetylglycine hydrazide

Chemical Property:

• Refractive Index: 1.8000 (estimate)
• Boiling Point: 281.77°C (rough estimate)
• PSA: 121.61000
• Density: 1.5005 (rough estimate)
• LogP: -1.04374
• XLogP3: -1.6
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 157.05997448
• Heavy Atom Count: 11
• Complexity: 207

Purity/Quality:

99% ^*data from raw suppliers

2-DIAZO-N-[(HYDRAZINECARBONYL)METHYL]ACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(=O)NN)NC(=O)C=[N+]=[N-]

Technology Process of Diazoacetylglycine hydrazide

There total 3 articles about Diazoacetylglycine hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-diazoacetyl)glycine ethyl ester (999-29-1) → N-diazoacetyl-glycine hydrazide (820-75-7)

Guidance literature:

With ethanol; hydrazine hydrate;

Reference yield:

N-(2-diazoacetyl)glycine ethyl ester (999-29-1) + ethanol (64-17-5) + hydrazine hydrate (7803-57-8,79785-97-0) → N-diazoacetyl-glycine hydrazide (820-75-7)

Guidance literature:

Bei kurzem Erwaermen;

Reference yield:

→ N-diazoacetyl-glycine hydrazide (820-75-7)

Guidance literature:

Diazoacetylglycin-aethylester, NH2-NH2;

DOI:10.1007/BF01990207

upstream raw materials:

N-(2-diazoacetyl)glycine ethyl ester

ethanol

hydrazine hydrate

Downstream raw materials:

hydrazine

N-diazoacetyl-glycine isopropylidenehydrazide