Technology Process of C36H37NO2S3
There total 4 articles about C36H37NO2S3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(R)-1-(4-isopropyl-2-thioxothiazolidin-3-yl)ethanone;
With
titanium tetrachloride;
In
dichloromethane;
at -78 ℃;
for 0.0833333h;
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at -78 ℃;
for 1h;
C28H24OS;
In
dichloromethane;
at -78 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hydroxide / tetrahydrofuran; water; ethanol / 2 h / 25 °C
2.1: diisobutylaluminium hydride / toluene / 1 h / 0 °C
3.1: N-ethyl-N,N-diisopropylamine; titanium tetrachloride / dichloromethane / 1.08 h / -78 °C
3.2: 1 h / -78 °C
With
titanium tetrachloride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1016/j.bmcl.2014.07.006
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / 0 °C
2.1: lithium hydroxide / tetrahydrofuran; water; ethanol / 2 h / 25 °C
3.1: diisobutylaluminium hydride / toluene / 1 h / 0 °C
4.1: N-ethyl-N,N-diisopropylamine; titanium tetrachloride / dichloromethane / 1.08 h / -78 °C
4.2: 1 h / -78 °C
With
carbon tetrabromide; titanium tetrachloride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1016/j.bmcl.2014.07.006
