Technology Process of C46H39BF2N4O4S2
There total 6 articles about C46H39BF2N4O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
piperidine;
In
chloroform; acetonitrile;
for 24h;
Reflux;
DOI:10.1039/c3ob40213d
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N-iodo-succinimide / dichloromethane / 12 h / 25 °C
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 12 h / Inert atmosphere; Reflux
3: N-iodo-succinimide / dichloromethane / 12 h / 25 °C
4: trichlorophosphate / ethylenediamine / 16 h / 25 °C / Cooling with ice
5: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 12 h / Inert atmosphere; Reflux
6: piperidine / acetonitrile; chloroform / 24 h / Reflux
With
piperidine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; chloroform; water; ethylenediamine; acetonitrile;
2: |Suzuki Coupling / 4: |Vilsmeier-Haack Formylation / 5: |Suzuki Coupling / 6: |Knoevenagel Condensation;
DOI:10.1039/c3ob40213d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-iodo-succinimide / dichloromethane / 12 h / 25 °C
2: trichlorophosphate / ethylenediamine / 16 h / 25 °C / Cooling with ice
3: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 12 h / Inert atmosphere; Reflux
4: piperidine / acetonitrile; chloroform / 24 h / Reflux
With
piperidine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; chloroform; water; ethylenediamine; acetonitrile;
2: |Vilsmeier-Haack Formylation / 3: |Suzuki Coupling / 4: |Knoevenagel Condensation;
DOI:10.1039/c3ob40213d