(S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

Base Information

Chemical Name:(S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether
CAS No.:104315-03-9
Molecular Formula:C₃₁H₃₀O₄
Molecular Weight:466.577
Hs Code.:

Synonyms:(S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

Suppliers and Price of (S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

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Technology Process of (S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

There total 5 articles about (S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 90-05-1
2-methoxy-phenol

: 104315-02-8
(R)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-ol

: 104315-03-9
(S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 2h;

Reference yield:

: 2930-05-4,14618-80-5,89616-40-0,16495-13-9
(S)-benzyl glycidyl ether

: 104315-03-9
(S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) sodium hydride / 1.) THF, 0 deg C, 30 min, 2.) THF, 0 deg C, 20 min

2: 100 percent / 30percent hydrogen peroxide / methanol; H₂O / 72 h / Ambient temperature

3: 1.) N,N,N',N'-tetramethylethylenediamine, 15percent n-butyl-lithium / 1.) THF, -55 deg C, n-hexane, r.t., 1 h, 2.) THF, 30 min, r.t.

4: calcium carbonate / toluene / 2 h / Heating

5: 48 percent / triphenylphosphine, di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; di-isopropyl azodicarboxylate; dihydrogen peroxide; sodium hydride; triphenylphosphine; calcium carbonate; In tetrahydrofuran; methanol; water; toluene;

Reference yield:

: 104314-99-0
(S)-1-benzyloxy-3-phenylthiopropan-2-ol

: 104315-03-9
(S)-(E)-1-benzyloxy-4-(4-benzyloxyphenyl)but-3-en-2-yl 2-methoxyphenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / 30percent hydrogen peroxide / methanol; H₂O / 72 h / Ambient temperature

2: 1.) N,N,N',N'-tetramethylethylenediamine, 15percent n-butyl-lithium / 1.) THF, -55 deg C, n-hexane, r.t., 1 h, 2.) THF, 30 min, r.t.

3: calcium carbonate / toluene / 2 h / Heating

4: 48 percent / triphenylphosphine, di-isopropyl azodicarboxylate / tetrahydrofuran / 2 h / 0 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine; calcium carbonate; In tetrahydrofuran; methanol; water; toluene;