4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid

Base Information

Chemical Name:4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid
CAS No.:888482-51-7
Molecular Formula:C₁₄H₁₃BrN₂O₃
Molecular Weight:337.173
Hs Code.:

Synonyms:4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid

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Chemical Property of 4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid

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Technology Process of 4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid

There total 1 articles about 4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 888482-53-9
4-(4-bromo-2-methyl-phenylamino)-6-chloro-nicotinic acid ethyl ester

: 74-88-4
methyl iodide

: 888482-51-7
4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid

Guidance literature:: 4-(4-bromo-2-methyl-phenylamino)-6-chloro-nicotinic acid ethyl ester; methyl iodide; In 1,2-dichloro-ethane; at 140 ℃; for 1.66667h; Irradiation;

With lithium hydroxide; at 140 ℃; for 0.166667h; Irradiation;

With formic acid; In methanol; dichloromethane;

Reference yield:

: 888482-51-7
4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid

: 4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid hydroxyamide

Guidance literature:: With hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 - 50 ℃; for 64h;

Reference yield:

: 888482-51-7
4-(4-bromo-2-methyl-phenylamino)-1-methyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid

: 120564-14-9
(S)-O-((2,2-dimethyl-1,3-dioxolan-4-yl)methyl)hydroxylamine

: C₂₀H₂₄BrN₃O₅

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 60 ℃; for 16h;