Technology Process of C59H101NO4
There total 3 articles about C59H101NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
chloroform;
for 48h;
DOI:10.1016/j.tet.2010.11.046
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ethanol; iron; ammonium chloride / 5 h / Reflux
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform / 48 h
With
ethanol; iron; ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
chloroform;
DOI:10.1016/j.tet.2010.11.046
- Guidance literature:
-
Multi-step reaction with 3 steps
1: nitric acid; acetic acid / dichloromethane / 2 h / 0 °C
2: ethanol; iron; ammonium chloride / 5 h / Reflux
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform / 48 h
With
ethanol; nitric acid; iron; ammonium chloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; chloroform;
DOI:10.1016/j.tet.2010.11.046