tert-butyl 2,6-dimethylbenzoperoxoate

Base Information

Chemical Name:tert-butyl 2,6-dimethylbenzoperoxoate
CAS No.:155249-15-3
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:222.284
Hs Code.:

Synonyms:tert-butyl 2,6-dimethylbenzoperoxoate

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Chemical Property of tert-butyl 2,6-dimethylbenzoperoxoate

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Technology Process of tert-butyl 2,6-dimethylbenzoperoxoate

There total 3 articles about tert-butyl 2,6-dimethylbenzoperoxoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 614-45-9
tert-Butyl peroxybenzoate

: 21900-37-8
2,6-dimethylbenzoyl chloride

: 155249-15-3
tert-butyl 2,6-dimethylbenzoperoxoate

Guidance literature:: tert-Butyl peroxybenzoate; With sodium hydride; In tetrahydrofuran; decane; mineral oil; at -10 ℃; for 0.333333h;

2,6-dimethylbenzoyl chloride; In tetrahydrofuran; decane; mineral oil; at -10 ℃; for 0.333333h;

Reference yield:

: 75-91-2
tert.-butylhydroperoxide

: 21900-37-8
2,6-dimethylbenzoyl chloride

: 155249-15-3
tert-butyl 2,6-dimethylbenzoperoxoate

Guidance literature:: tert.-butylhydroperoxide; With sodium hydride; In tetrahydrofuran; decane; mineral oil; at -10 ℃; for 0.333333h; Inert atmosphere; Sealed tube;

2,6-dimethylbenzoyl chloride; In tetrahydrofuran; decane; mineral oil; at -10 ℃; for 0.333333h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.1c02215

Reference yield:

: 632-46-2
2,6-dimethylbenzoic acid

: 155249-15-3
tert-butyl 2,6-dimethylbenzoperoxoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 0 - 20 °C / Sealed tube; Inert atmosphere

2.1: sodium hydride / decane; tetrahydrofuran; mineral oil / 0.33 h / -10 °C / Inert atmosphere; Sealed tube

2.2: 0.33 h / -10 °C / Inert atmosphere; Sealed tube

With oxalyl dichloride; sodium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; decane; dichloromethane; mineral oil;
DOI:10.1021/acs.orglett.1c02215