2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran

Base Information

Chemical Name:2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran
CAS No.:104794-83-4
Molecular Formula:C₂₆H₂₆N₄O₆
Molecular Weight:490.516
Hs Code.:

Synonyms:2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran

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Chemical Property of 2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran

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Technology Process of 2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran

There total 5 articles about 2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 24170-23-8
3-nitro-4-acetylaminobenzoyl chloride

: 104794-81-2
4-Phenyl-2,5-dimethyl-3-(piperazinocarbonyl)furan

: 104794-83-4
2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran

Guidance literature:: With triethylamine; In benzene; at 30 ℃; for 2h;

Reference yield:

: 104794-30-1
3-Carboxy-2,5-dimethyl-4-phenylfuran

: 104794-83-4
2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / benzene / 3 h / Heating

2: triethylamine / benzene / 2 h / 30 °C

3: 80 percent / NaOH / ethanol; H₂O / 4 h / Heating

4: 65 percent / triethylamine / benzene / 2 h / 30 °C

With sodium hydroxide; thionyl chloride; triethylamine; In ethanol; water; benzene;

Reference yield:

: 17168-38-6
2,5-dimethyl-4-phenylfuran-3-carboxylic acid methylester

: 104794-83-4
2,5-Dimethyl-3-<4-(3-nitro-4-acetamidobenzoyl)-piperazinocarbonyl>-4-phenylfuran

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / KOH / H₂O; methanol / 4 h / Heating

2: thionyl chloride / benzene / 3 h / Heating

3: triethylamine / benzene / 2 h / 30 °C

4: 80 percent / NaOH / ethanol; H₂O / 4 h / Heating

5: 65 percent / triethylamine / benzene / 2 h / 30 °C

With potassium hydroxide; sodium hydroxide; thionyl chloride; triethylamine; In methanol; ethanol; water; benzene;