C₁₃H₁₈O₄S

Base Information

Chemical Name:C₁₃H₁₈O₄S
CAS No.:1422044-12-9
Molecular Formula:C₁₃H₁₈O₄S
Molecular Weight:270.35
Hs Code.:

C<sub>13</sub>H<sub>18</sub>O<sub>4</sub>S

Synonyms:C₁₃H₁₈O₄S

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Chemical Property of C₁₃H₁₈O₄S

Chemical Property:

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Technology Process of C₁₃H₁₈O₄S

There total 4 articles about C₁₃H₁₈O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 115369-27-2
R-1-(benzenesulfonyl)-butane-3,4-diol

: 77-76-9
2,2-dimethoxy-propane

: 1422044-12-9
C₁₃H₁₈O₄S

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 14h;
DOI:10.1021/ol303272w

Reference yield:

: 67100-44-1
(but-3-en-1-ylsulfonyl)benzene

: 1422044-12-9
C₁₃H₁₈O₄S

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 48 h / 20 °C

2: (S,S)-(+)-N,N’-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminomanganese(III) chloride / toluene; acetic acid; tetrahydrofuran; water / 18 h / 0 - 20 °C

3: toluene-4-sulfonic acid / dichloromethane / 14 h / 20 °C

With (S,S)-(+)-N,N’-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminomanganese(III) chloride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water; acetic acid; toluene;
DOI:10.1021/acs.joc.6b00900

Reference yield:

: 873-55-2
sodium benzenesulfonate

: 1422044-12-9
C₁₃H₁₈O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 5 h / 20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 48 h / 20 °C

3: (S,S)-(+)-N,N’-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminomanganese(III) chloride / toluene; acetic acid; tetrahydrofuran; water / 18 h / 0 - 20 °C

4: toluene-4-sulfonic acid / dichloromethane / 14 h / 20 °C

With (S,S)-(+)-N,N’-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediaminomanganese(III) chloride; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; toluene;
DOI:10.1021/acs.joc.6b00900