1-(trifluoromethyl)-3-butenyl phenylsulfide

Base Information

Chemical Name:1-(trifluoromethyl)-3-butenyl phenylsulfide
CAS No.:129286-67-5
Molecular Formula:C₁₁H₁₁F₃S
Molecular Weight:232.27
Hs Code.:

Synonyms:1-(trifluoromethyl)-3-butenyl phenylsulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(trifluoromethyl)-3-butenyl phenylsulfide

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Technology Process of 1-(trifluoromethyl)-3-butenyl phenylsulfide

There total 3 articles about 1-(trifluoromethyl)-3-butenyl phenylsulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5296-64-0
allyl phenyl thioether

: 2236129-81-8
trifluoroacetaldehyde N-triftosylhydrazone

: 129286-67-5
1-(trifluoromethyl)-3-butenyl phenylsulfide

Guidance literature:: With 5,10,15,20-tetraphenyl iron porphyrin; sodium hydroxide; In dichloromethane; at 40 ℃; Inert atmosphere;

Reference yield: 81.0%

: 114953-71-8,129286-61-9
[(1-chloro-2,2,2-trifluoroethyl)sulfanyl]benzene

: 762-72-1
allyl-trimethyl-silane

: 129286-67-5
1-(trifluoromethyl)-3-butenyl phenylsulfide

Guidance literature:: With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; Heating;
DOI:10.1021/jo00306a013

Reference yield:

: 2262-07-9
2,2,2-trifluoroethyl phenyl sulfide

: 129286-67-5
1-(trifluoromethyl)-3-butenyl phenylsulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / SO₂Cl₂ / hexane / Ambient temperature

2: 81 percent / BF₃*OEt₂ / 1,2-dichloro-ethane / Heating

With sulfuryl dichloride; boron trifluoride diethyl etherate; In hexane; 1,2-dichloro-ethane;
DOI:10.1021/jo00306a013