C₂₄H₃₈O₈

Base Information

Chemical Name:C₂₄H₃₈O₈
CAS No.:1442433-49-9
Molecular Formula:C₂₄H₃₈O₈
Molecular Weight:454.561
Hs Code.:

C<sub>24</sub>H<sub>38</sub>O<sub>8</sub>

Synonyms:C₂₄H₃₈O₈

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Chemical Property of C₂₄H₃₈O₈

Chemical Property:

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Technology Process of C₂₄H₃₈O₈

There total 19 articles about C₂₄H₃₈O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1442433-47-7
(6S,9S,10S,E)-10-((4-methoxybenzyl)oxy)-6,9-bis(methoxymethoxy)oxacyclotridec-7-en-2-one

: 1442433-49-9
C₂₄H₃₈O₈

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.04.069

Reference yield:

: 1007401-44-6
((2S,3S)-2-(4-(tert-butyldiphenylsilyloxy)butyl)oxiran-2-yl)methanol

: 1442433-49-9
C₂₄H₃₈O₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 0.17 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / 2 h / 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C

5.1: sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogenphosphate / tetrahydrofuran; tert-butyl alcohol; water / 3 h / 0 - 20 °C

6.1: dmap; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 0 °C

6.2: 12 h / 0 - 20 °C

7.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 36 h / Inert atmosphere; Reflux

8.1: diisobutylaluminium hydride / dichloromethane; toluene / -78 - 0 °C / Inert atmosphere

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; iodine; diisobutylaluminium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2013.04.069

Reference yield:

: 1442433-46-6
(S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

: 1442433-49-9
C₂₄H₃₈O₈

Guidance literature:: Multi-step reaction with 2 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 36 h / Inert atmosphere; Reflux

2: diisobutylaluminium hydride / dichloromethane; toluene / -78 - 0 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; diisobutylaluminium hydride; In dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.04.069