2-[4-(5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione

Base Information

• Chemical Name: 2-[4-(5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione
• CAS No.: 106834-32-6
• Molecular Formula: C₂₃H₁₉N₂O₈P
• Molecular Weight: 482.386

Synonyms:2-[4-(5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione

Chemical Property of 2-[4-(5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione

Chemical Property:

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Technology Process of 2-[4-(5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione

There total 2 articles about 2-[4-(5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

4-nitronaphthalic-1,8-anhydride (6642-29-1) + p-aminophenyl 2,2-dimethyltrimethylene phosphate (106834-29-1) → 2-[4-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione (106834-32-6)

Guidance literature:

In acetic acid; for 2h; Heating;

Reference yield:

2,2-dimethyltrimethylene p-nitrophenyl phosphate (1028-00-8) → 2-[4-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione (106834-32-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 55 percent /

2: 69 percent / acetic acid / 2 h / Heating

With ; In acetic acid;

Reference yield: 53.5%

2-[4-(5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-6-nitro-benzo[de]isoquinoline-1,3-dione (106834-32-6) → 6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione (106834-35-9)

Guidance literature:

With hydrazine hydrate; nickel; In ethanol; for 7h; Heating;

upstream raw materials:

4-nitronaphthalic-1,8-anhydride

p-aminophenyl 2,2-dimethyltrimethylene phosphate

2,2-dimethyltrimethylene p-nitrophenyl phosphate

Downstream raw materials:

6-Amino-2-[4-(5,5-dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-yloxy)-phenyl]-benzo[de]isoquinoline-1,3-dione

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