tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate

Base Information

Chemical Name:tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate
CAS No.:737784-49-5
Molecular Formula:C₂₃H₃₁ClN₂O₃
Molecular Weight:418.964
Hs Code.:

Synonyms:tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate

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Chemical Property of tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate

Chemical Property:

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Technology Process of tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate

There total 1 articles about tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 214957-13-8
2-amino-5-chloro-α-(3-tert-butoxycarbonylaminomethylphenyl)benzyl alcohol

: 78-84-2
isobutyraldehyde

: 737784-49-5
tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate

Guidance literature:: 2-amino-5-chloro-α-(3-tert-butoxycarbonylaminomethylphenyl)benzyl alcohol; isobutyraldehyde; With acetic acid; In methanol; at 20 ℃; for 1h;

With sodium cyanoborohydride; In methanol; at 20 ℃; for 24h;

Reference yield:

: 737784-49-5
tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate

: 26367-48-6
fumaric acid ethyl ester mono chloride

: ethyl [3,5-trans-5-[3-(tert-butoxycarbonylaminomethyl)phenyl]-7-chloro-1-isobutyl-2-oxo-1,2,3,5-tetrahydro-4,1-benzoxazepin-3-yl]acetate

Guidance literature:: tert-butyl [3-[[5-chloro-2-(isobutylamino)phenyl](hydroxy)methyl]benzyl]carbamate; fumaric acid ethyl ester mono chloride; With sodium hydrogencarbonate; In water; ethyl acetate; at 20 ℃; for 2h;

With potassium carbonate; In ethanol; at 60 ℃; for 2h;