Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester

Base Information

Chemical Name:Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester
CAS No.:200813-12-3
Molecular Formula:C₁₅H₁₃F₃N₂O₃
Molecular Weight:326.275
Hs Code.:

Synonyms:Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester

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Technology Process of Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester

There total 1 articles about Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-56-1
methanol

: 179996-84-0
1-Methyl-5-phenyl-7-trifluoromethyl-1H-oxazolo[5,4-b]pyridin-2-one

: 200813-12-3
Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester

Guidance literature:: With potassium hydroxide; for 2h; Heating;
DOI:10.1007/BF02256763

Reference yield: 87.8%

: 200813-12-3
Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester

: 179996-84-0
1-Methyl-5-phenyl-7-trifluoromethyl-1H-oxazolo[5,4-b]pyridin-2-one

Guidance literature:: With triethylamine; In N,N-dimethyl acetamide; for 1h; Heating;
DOI:10.1007/BF02290731

Reference yield:

: 200813-12-3
Methyl-(2-oxo-6-phenyl-4-trifluoromethyl-1,2-dihydro-pyridin-3-yl)-carbamic acid methyl ester

: N'-benzyl-N-methyl-N-(2-oxo-4-trifluoromethyl-6-phenyl-3-pyridyl)urea

Guidance literature:: Multi-step reaction with 2 steps

1: 87.8 percent / triethylamine / N,N-dimethyl-acetamide / 1 h / Heating

2: 64.7 percent / dioxane / 6 h / 95 - 100 °C

With triethylamine; In 1,4-dioxane; N,N-dimethyl acetamide; 1: Cyclization / 2: Ring cleavage;
DOI:10.1007/BF02290731