(1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Base Information

• Chemical Name: (1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione
• CAS No.: 959911-30-9
• Molecular Formula: C₂₂H₂₄N₂O₃
• Molecular Weight: 364.444

Synonyms:(1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Chemical Property of (1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

Chemical Property:

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Technology Process of (1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione

There total 1 articles about (1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

benzyl bromide (100-39-0) + (1S,5S)-6-benzyl-2-methoxy-8-methyl-6.8-diazabicyclo[3.2.2]nonane-2,7,9-trione (269717-68-2) → (1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (959911-30-9) + (1S,2S,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (959911-29-6)

Guidance literature:

(1S,5S)-6-benzyl-2-methoxy-8-methyl-6.8-diazabicyclo[3.2.2]nonane-2,7,9-trione; With sodium tetrahydroborate; In tetrahydrofuran; propan-1-ol; water; at 20 ℃; for 16h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 20 ℃; for 16h; Further stages.;

DOI:10.1016/j.ejmech.2007.02.005

Reference yield: 63.0%

(1S,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane-7,9-dione (959911-30-9) → (1R,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane (959911-36-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 66 ℃; for 50h;

DOI:10.1016/j.ejmech.2007.02.005

upstream raw materials:

benzyl bromide

(1S,5S)-6-benzyl-2-methoxy-8-methyl-6.8-diazabicyclo[3.2.2]nonane-2,7,9-trione

Downstream raw materials:

(1R,2R,5S)-6-benzyl-2-benzyloxy-8-methyl-6,8-diazabicyclo[3.2.2]nonane

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