allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside

Base Information

Chemical Name:allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside
CAS No.:1245641-29-5
Molecular Formula:C₃₇H₄₂O₁₆
Molecular Weight:742.731
Hs Code.:

Synonyms:allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside

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Chemical Property of allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside

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Technology Process of allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside

There total 7 articles about allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1245641-25-1
allyl 2,3-di-O-benzoyl-α-L-fucopyranoside

: 86520-63-0
2,3,4,6-tetra-O-acetyl-α-galactopyranosyl trichloroacetimidate

: 1245641-29-5
allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1248/cpb.58.495

Reference yield:

: 3646-73-9
α-D-galactopyranose

: 1245641-29-5
allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: indium(III) triflate

2: hydrazinium monoacetate

3: 1,8-diazabicyclo[5.4.0]undec-7-ene

4: indium(III) triflate

With indium(III) triflate; hydrazinium monoacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene;
DOI:10.1021/acs.biomac.1c01001

Reference yield:

: 41308-77-4
allyl α-L-fucopyranoside

: 1245641-29-5
allyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-α-L-fucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid

2: pyridine

3: acetyl chloride; methanol

4: indium(III) triflate

With indium(III) triflate; pyridine; methanol; toluene-4-sulfonic acid; acetyl chloride;
DOI:10.1021/acs.biomac.1c01001