Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester

Base Information

• Chemical Name: Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester
• CAS No.: 67886-47-9
• Molecular Formula: C₂₁H₂₇O₆PS
• Molecular Weight: 438.482

Synonyms:Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester

Chemical Property of Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester

Chemical Property:

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Technology Process of Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester

There total 2 articles about Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid methyl ester (93-58-3,5705-52-2,80226-58-0) → Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester (67886-47-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) nBuLi, HMPT, hexane, THF, (ii) /BRN= 1072099/

2: (i) KH, HMPT, THF, (ii) /BRN= 471433/

DOI:10.1021/ja00483a035

Reference yield:

butyl phenyl sulfone (16823-62-4) → Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester (67886-47-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) nBuLi, HMPT, hexane, THF, (ii) /BRN= 1072099/

2: (i) KH, HMPT, THF, (ii) /BRN= 471433/

DOI:10.1021/ja00483a035

Reference yield:

Phosphoric acid (Z)-2-benzenesulfonyl-1-phenyl-pent-1-enyl ester diethyl ester (67886-47-9) → 1-phenyl-1-pentyne (4250-81-1)

Guidance literature:

With sodium amalgam; In tetrahydrofuran;

DOI:10.1021/ja00483a035

upstream raw materials:

benzoic acid methyl ester

butyl phenyl sulfone

Downstream raw materials:

1-phenyl-1-pentyne

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