Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂

Base Information

Chemical Name:Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂
CAS No.:1253784-30-3
Molecular Formula:C₅₈H₅₂O₆P₂Pt
Molecular Weight:1102.07
Hs Code.:

Pt(PPh<SUB>3</SUB>)<SUB>2</SUB>(CCC<SUB>6</SUB>H<SUB>2</SUB>(OMe)<SUB>3</SUB>-3,4,5)<SUB>2 </SUB>

Synonyms:Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂

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Chemical Property of Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂

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Technology Process of Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂

There total 2 articles about Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 53560-33-1
3,4,5-trimethoxyphenylacetylene

: 1253784-30-3
trans-[Pt(triphenylphosphine)2(3,4,5-trimethoxyphenylethynyl)2]

Guidance literature:: copper(l) iodide; In diethylamine; under N2; Pt complex dissolved in HNEt2 contg. CuI; ligand added; heatedto reflux for 8 h with stirring; modified from S. Leininger, P. J. Stra ng, S. Huang, Organometallics, 1998, 17, 3981; filtered; solvent removed under reduced pressure; dissolved in CH2Cl2; ;washed successively with NH4Cl soln. and deionized H2O; org. layer drie d (anhyd. MgSO4); filtered; concd. under reduced pressure; recrystd. from CH2Cl2-Et2O; elem. anal.;
DOI:10.1021/om100473q

Reference yield:

: 10199-34-5,14056-88-3,15604-36-1
bis(triphenylphosphine)platinum(II) dichloride

: 53560-33-1
3,4,5-trimethoxyphenylacetylene

: 1253784-30-3
Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂

Guidance literature:: With copper(l) iodide; triethylamine; In chloroform; at 50 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic4000457

Reference yield: 86.0%

: Ag(tetrahydrothiophene)ClO₄

: 1253784-30-3
Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂

: 2071-24-1
bis(diphenylphosphinomethyl)phenylphosphine

: [PtAg₂(bis(diphenylphosphinomethyl)phenylphosphine)₂(1-ethynyl-3,4,5-trimethoxybenzene^(1-))₂](perchlorate)₂

Guidance literature:: Ag(tetrahydrothiophene)ClO₄; bis(diphenylphosphinomethyl)phenylphosphine; In dichloromethane; for 0.5h; Inert atmosphere; Schlenk technique;

Pt(PPh₃)₂(CCC₆H₂(OMe)₃-3,4,5)₂; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic4000457