Cyclohexyl-trimethylsilanyloxy-methanethiol

Base Information

Chemical Name:Cyclohexyl-trimethylsilanyloxy-methanethiol
CAS No.:78371-38-7
Molecular Formula:C₁₀H₂₂OSSi
Molecular Weight:218.436
Hs Code.:

Synonyms:Cyclohexyl-trimethylsilanyloxy-methanethiol

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Chemical Property of Cyclohexyl-trimethylsilanyloxy-methanethiol

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Technology Process of Cyclohexyl-trimethylsilanyloxy-methanethiol

There total 4 articles about Cyclohexyl-trimethylsilanyloxy-methanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 75-77-4
chloro-trimethyl-silane

: 2043-61-0
cyclohexanecarbaldehyde

: 78371-38-7
Cyclohexyl-trimethylsilanyloxy-methanethiol

Guidance literature:: With pyridine; hydrogen sulfide; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.201802845

Reference yield:

: C₂₆H₅₄O₂S₂Si₂

: 78371-38-7
Cyclohexyl-trimethylsilanyloxy-methanethiol

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide; aq. phosphate buffer / 13 h / 20 °C / pH 5

2: pyridine; hydrogen sulfide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With pyridine; hydrogen sulfide; In aq. phosphate buffer; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201802845

Reference yield:

: C₁₃H₂₇NO₂SSi

: 78371-38-7
Cyclohexyl-trimethylsilanyloxy-methanethiol

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / dichloromethane; methanol; water

2: pyridine; hydrogen sulfide / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With pyridine; hydrogenchloride; hydrogen sulfide; In methanol; dichloromethane; water;
DOI:10.1002/anie.201802845