N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

Base Information

Chemical Name:N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester
CAS No.:114340-57-7
Molecular Formula:C₃₂H₄₈N₄O₇
Molecular Weight:600.756
Hs Code.:

Synonyms:N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

Suppliers and Price of N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

There total 4 articles about N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 114340-53-3
2-tert-butyl-1,3-di-N-(hydroxyl) succinimidyl citrate

: 84627-29-2
N-benzyloxy-1,4-diaminobutane dihydrochloride

: 114340-57-7
N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

Guidance literature:: With triethylamine; In 1,4-dioxane; for 2.5h;

Reference yield:

: 53798-96-2
1,5-dimethyl citrate

: 114340-57-7
N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 63 percent / HClO₄ / 72 h

2: 82 percent / 2 M NaOH / methanol; H₂O / 3 h

3: 85 percent / DCCI / dioxane; ethyl acetate / 15 h

4: 90 percent / Et₃N / dioxane / 2.5 h

With sodium hydroxide; perchloric acid; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; methanol; water; ethyl acetate;

Reference yield:

: 114340-52-2
3-(tert-butoxycarbonyl)-3-hydroxypentanedioic acid

: 114340-57-7
N-(4-Benzyloxyamino-butyl)-2-[(4-benzyloxyamino-butylcarbamoyl)-methyl]-2-hydroxy-succinamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / DCCI / dioxane; ethyl acetate / 15 h

2: 90 percent / Et₃N / dioxane / 2.5 h

With triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; ethyl acetate;