(2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate

Base Information

Chemical Name:(2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate
CAS No.:1071476-37-3
Molecular Formula:C₁₇H₂₅NO₄S
Molecular Weight:339.456
Hs Code.:

Synonyms:(2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate

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Chemical Property of (2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate

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Technology Process of (2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate

There total 3 articles about (2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 914094-53-4
2-(3-(bromomethyl)phenoxy)tetrahydro-2H-pyran

: 85950-53-4
D-cysteine ethyl ester

: 1071476-37-3
(2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate

Guidance literature:: 2-(3-(bromomethyl)phenoxy)tetrahydro-2H-pyran; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;

D-cysteine ethyl ester; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 1071476-37-3
(2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane / 5 - 12 h / 20 °C

2.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2.2: 12 h / 20 °C

With pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 74597-04-9
m-hydroxybenzyl bromide

: 1071476-37-3
(2S)-ethyl 2-amino-3-(3-(tetrahydro-2H-pyran-2-yloxy)benzylthio)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane / 5 - 12 h / 20 °C

2.1: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2.2: 12 h / 20 °C

With pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;