(5Z,9α,11α,13E)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid

Base Information

• Chemical Name: (5Z,9α,11α,13E)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid
• CAS No.: 41691-84-3
• Molecular Formula: C₂₁H₃₆O₅
• Molecular Weight: 368.514

Synonyms:(5Z,9α,11α,13E)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid

Chemical Property of (5Z,9α,11α,13E)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of (5Z,9α,11α,13E)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid

There total 2 articles about (5Z,9α,11α,13E)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (Z)-7-[(1R,3R,5S)-3,5-Dihydroxy-2-((E)-(R)-3-hydroxy-3-methyl-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid (35700-23-3,35700-24-4,35700-25-5,35864-81-4,41691-84-3,59286-19-0,62446-63-3,62776-95-8,68906-67-2,68906-68-3,76498-29-8,80124-57-8,90695-58-2,90695-59-3,100019-29-2,113626-85-0)

Guidance literature:

15-Oxo-1,9,11-tris-OSi(Me)3-PGF(2α), 1.) MeMgBr, 2.) W.;

Reference yield:

→ (Z)-7-[(1R,3R)-3,5-Dihydroxy-2-((E)-(S)-3-hydroxy-3-methyl-oct-1-enyl)-cyclopentyl]-hept-5-enoic acid (35700-23-3,35700-24-4,35700-25-5,35864-81-4,41691-84-3,59286-19-0,62446-63-3,62776-95-8,68906-67-2,68906-68-3,76498-29-8,80124-57-8,90695-58-2,90695-59-3,100019-29-2,113626-85-0)

Guidance literature:

TMS-Derivat v. 15-Oxo-PGF(2β) u. CH3MgBr;

Reference yield: 57.5%

(5Z,9α,11α,13E)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid (41691-84-3) + methyl iodide (74-88-4) → U 36384 (35700-21-1) + (5Z,9α,11α,13E,15R)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid methyl ester (35700-22-2)

Guidance literature:

With potassium carbonate; In acetone; at 50 ℃; Large scale;

Downstream raw materials:

U 36384

(5Z,9α,11α,13E,15R)-15-methyl-9,11,15-trihydroxy-prosta-5,13-diene-1-carboxylic acid methyl ester

Carboprost

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