3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester

Base Information

Chemical Name:3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester
CAS No.:239807-64-8
Molecular Formula:C₂₁H₃₅N₃O₃
Molecular Weight:377.527
Hs Code.:

Synonyms:3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester

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Chemical Property of 3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester

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Technology Process of 3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester

There total 3 articles about 3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 54013-91-1
2-(1-methylethoxy)phenyl-1-piperazine

: 239807-64-8
3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester

Guidance literature:: With caesium carbonate; In acetonitrile; Heating;
DOI:10.1021/jm9905918

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 239807-64-8
3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / CH₂Cl₂ / 4 h / 20 °C

2: 81 percent / Cs₂CO₃ / acetonitrile / Heating

With caesium carbonate; In dichloromethane; acetonitrile; 1: Acylation / 2: Alkylation;
DOI:10.1021/jm9905918

Reference yield:

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 119695-87-3
fumarate salt of 4-(2-isopropyloxyphenyl)piperazine

: 239807-64-8
3-[4-[2-(1-methylethoxy)phenyl]-1-piperazinyl]propylcarbamic acid, 1,1-dimethylethyl ester

Guidance literature:: fumarate salt of 4-(2-isopropyloxyphenyl)piperazine; With sodium hydroxide; In water;

3-bromopropylamine tert-butylcarbamate; With caesium carbonate; In acetonitrile; Heating / reflux;