2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one

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Chemical Name:2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one
CAS No.:1227738-15-9
Molecular Formula:C₃₇H₃₉N₃O₉
Molecular Weight:669.731
Hs Code.:

Synonyms:2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one

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Chemical Property of 2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one

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Technology Process of 2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one

There total 9 articles about 2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1272644-76-4
2-(4-(3-bromopropoxy)-3-methoxyphenyl)-2,3-dihydroquinazolin-4(1H)-one

: 2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenol

: 1227738-15-9
2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2010.12.004

Reference yield:

: 108012-55-1
2-(4-hydroxy-3-methoxyphenyl)-2,3-dihydroquinazolin-4(1H)-one

: 1227738-15-9
2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2010.12.004

Reference yield:

: 39201-89-3
3,4,5-trimethoxybenzaldehyde oxime

: 1227738-15-9
2-(3-methoxy-4-(3-(2-methoxy-5-(3-(3,4,5-trimethoxyphenyl)-4,5-dihydroisoxazol-5-yl)phenoxy)propoxy)phenyl)-2,3-dihydroquinazolin-4(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hypochlorite; triethylamine / dichloromethane; water / 25 h / 0 - 20 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

2.2: 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

With sodium hypochlorite; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2010.12.004